Open Access Open Access  Restricted Access Subscription or Fee Access

Characterization of Pure and Ag Doped ZnO Nanostructure and Study the Effect of Calcination Temperature on Bacterial Growth of Ag Doped ZnO Nanostructure.

Limbraj Sopan Rvangave, Shaikh R S

Abstract


Sol-Gel chemical precipitation method has been implemented to synthesize Ag doped ZnO nanoparticles at 50°C. Wurtzite hexagonal crystal structure of pure and ZnO(Ag) nanoparticles have been confirmed by X-ray Diffraction (XRD) data. The crystalline size and have been estimated using XRD data. The chemical composition of pure and Ag doped ZnO nanoparticles has been investigated by analysis of Fourier transform infrared (FTIR) spectroscopy. The direct band gap of nanoparticles has been estimated using optical absorption spectra. Defects due to oxygen deficiency and interstitial vacancy have been confirmed using Photoluminescence (PL) spectra. The effect of calcination temperature of ZnO(Ag) on antimicrobial activity of Bacillus thuringiensis NCIM2130 and Pseudomonas cf. monteilii 9 have been investigated.

Keywords: ZnO nanoparticles, XRD spectra, PL spectra, optical band gap, Antibacterial activity.


Full Text:

PDF

References


Esmailzadeh H, Sang PP, Khaksar R, et al. Effects of Zinc Oxide Nanoparticles on the Growth of Bacillus subtilis and E. coli 0157:H7. Journal of Food Technology and Nutrition 2014; 11(3): 21–28p.

Emami FA, Kadivar M, Shahedi M, et al. Effect of Nanocomposite Packaging Containing Silver and Zinc Oxide on the Shelf Life of Fresh Orange Juice. Journal of Nutrition Sciences & Food Technology. 2011; 6, 1(20): 57–67p.

Veissi MZ Afshar D, Ranjbar R, et al. Antimicrobial Properties of ZnO Nanoparticles. J MDPI Tropical Med. 2012; 17(59): 1–4p.

Emanetoglu NW, Gorla C, Liu Y, et al. Epitaxial ZnO Piezoelectric Thin Films for Saw Filters. Materials Sci in Semicond Processing. 1999; 2(3): 247–252p.

Chen Y, Bagnall D, Yao T. ZnO as a Novel Photonic Material for the UV Region. Mater Sci Eng B. 2000; 75(2–3): 190–198p.

Characterization of Pure and Ag Doped ZnO and Effect of Calcinations of on (Ag) Ravangve and Shaikh

JoNSNEA (2018) 31-38 © STM Journals 2018. All Rights Reserved Page 38

Mitra P, Chatterjee AP, Maiti HS. ZnO Thin Film Sensor. Mater Lett. 1998; 35(1– 2): 33–38p.

Sharma N, Kumar J, Thakur S, et al. Antibacterial Study of Silver Doped Zinc Oxide Nanoparticles against Staphylococcus aureus and Bacillus subtilis. Drug Invention Today (DIT). 2013; 5: 50–54p.

Navale GR, Thripuranthaka M, Late DJ, et al. Antimicrobial Activity of ZnO Nanoparticles against Pathogenic Bacteria and Fungi. JSM Nanotechnol Nanomed. 2015; 3(1): 1033–39p.

Zhang H, Feng J, Wong J. Preparation of ZnO Nanorods through Wet Chemical Precipitation Method. J Mater Lett. 2007; 61(30): 5202–5205p. 10. . Purwaning Sinh SY, Pratapa S. Synthesis of Nanosized ZnO Particles by Co- Precipitation Method with Variation of Heating Time. API Conference Proceedings. 2016; 1710(1).

Chang P, Forn Z, Wong D. ZnO Nanowires Synthesized by Vapour Trapping CVD Method. J Chem Mater. 2004; 16(24): 5133–5137p.

Kumar A, Karimi NA. Synthesis of Zinc Oxide Nanoparticles by Sol-Gel Method. Informatics J. 2015; 31(3–4).

He S, Zhang M, Yao L. Preparation and Properties of ZnO Nanostructures by Electrochemical Anodization Mehod. Appl Surf Sci. 2010; 256(8): 2557–2562p.

Evi Mayanti, Sal Prima, Yudha S. Synthesis of ZnO Nanoparticles by Hydrothermal Method. Mater Lett. 2014; 118: 96–98p.

Sikwal NR, Sonwane SH. Ultrasound – Assisted Preparation of ZnO Nanostructures. Green Processing and Synthesis. 2016; 5(2): 163–172p. 16. Vidyasagar CC, Khanfounch, Mohmad. Microwave Combustion Synthesis of Cr- ZnO Nanocrystal. J Adv Sci. 2017; 9(10): 810–815p.

Cullity BD, Stock SR. Elements of X-Ray Diffraction. 3rd Edn. New Jersey: Prentice Hall; 2001.

Buerger MJ. X-ray Crystallography. 3rd Edn. New York: John Wiley and Sons; 1962.

Pal B, Giri PK. Defect Mediated Magnetic Interaction and High Tc Ferromagnetism in Co Doped ZnO Nanoparticles. J Nanosci Nanotechnol. 2011; 11(10): 1–8p.

Kwon YJ, Kim KH, Lim CS. Characterization of ZnO Nanopowder Synthesized by the Polymerized Complex Method via an Organochemical Route. J Ceram Proc Res. 2002; 3: 146–149p.

Silva RF, Zaniquelli MED. Morphology of Nanometric Size Particulate Aluminium Doped Zinc Oxide Films. Colliod Surf Physicochem Eng Aspect. 2002; 198–200: 551–558p.

Li H, Wang J, Liu H. Sol-Gel Preparation of Transparent Zinc Oxide Films with Highly Preferential Crystal Orientation. Vacuum. 2004; 77(1): 57–62p.

Farzane H, Dowlatababdi Gholamreza A, Maryam MS. Investigation of the Antimicrobial Effect of Silver Doped Zinc Oxide Nanoparticles. Nanomed J. 2017; 4(1): 50–54p.

Udaykumar S, Renuga V, Kavitha K. Synthesis and Characterization of Ni- Doped ZnO by Chemical Precipitation Method. Int J Sci Res. 2012; 3(2): 118– 122p.

Jiang L, Wang F, Han F, et al. Evaluation of Diffusion and Dilution Methods to Determine the Antimicrobial Activity of Water-Soluble Chitosan Derivatives. J Appl Microbiol. 2012; 114(4): 956–963p.

Balouiri M, Sadiki M, Ibnsouda SK. Methods for in vitro Evaluating Antimicrobial Activity: A Review. J Pharm Anal. 2016; 6(2): 71–79p.


Refbacks

  • There are currently no refbacks.